TOKYO RIKAKIKAI CO., LTD. 個人有機合成化學工作站 反應容器數量: 1 ~ 4 PPV-5460 PPV-5460

Feature

• Adjustable Size for Separable Flasks
• A space-saving synthetic device designed for general liquid-phase organic chemistry experiments. Four types of experiments can be carried out at once by combining the types and sizes of reaction vessels. This enables efficient research on new reactions, development of new catalysts, and examination of reaction conditions. It is equipped with individual temperature control function by aluminum block thermostatic bath and stirring function by strong magnetic force magnetic stirrer.
• The size of the reactor can be changed by replacing the test tube adapter. Experiments can be performed in a wide range of synthetic scales of 11~150 mL. Can be used in combination with a glass reactor and a stainless steel reactor.
• Small separable flasks can also be used. Since it has a large diameter, it can be easily prepared, curetted and washed. You can select from 4 types, size and number of units, depending on the application.
• Each of the four heating blocks is equipped with a temperature sensor and a temperature controller. Temperature control can be started/stopped and temperature can be set for each reactor. Due to the constant flow of cooling water, if the temperature control is stopped after a high temperature reaction, the water will cool down rapidly, making it difficult to overreact.
• Each of the four reactor vessels is equipped with a ferromagnetic driving magnet, which provides strong and reliable stirring. The four driving shafts are controlled by a single motor for stable rotation adjustment from low speed to high speed. Reaction experiments using poorly soluble powder reagents and solid catalysts are also possible.

Specifications

• Stirring method: Ferromagnetic magnetic stirrer
• Performance:
• Number of reaction vessels: 1 ~ 4
• Synthetic scale: 11 ~ 150 mL (depends on the reaction vessel used) * Reaction vessel related parts are sold separately.
• Temperature control range (aluminum block temperature): - 27 ~ 200 C (4 x individual temperature control) * A cooling water circulator is required.
• Temperature control accuracy: +/- 0.5 degrees C
• Rotating speed range: 50 ~ 900 rpm (with water)
• Features:
• Temperature setting and display: Sheet key input and digital display (- 40.0 ~ 200.0 C)
• Stirring setting and display: Volume setting and digital display (20 ~ 2000 rpm)
• Gas replacement: by vacuum drawing + inert gas introduction (depending on container)
• Refluxing: High-efficiency refluxing with a Jimlott cooling tube
• Method of adding reagents: pipette, syringe, dropping funnel (manual addition)
• Reaction observation: By slit in aluminum block (with lighting)
• Safety features: Leakage/overcurrent breaker, temperature fuse, temperature controller self-diagnostic function (Variable Upper Temperature, Fixed Upper Temperature, Sensor Abnormal), defrost heater, double chamber, drop tray, motor overload protection
• Standard:
• Wetted Part Material: Glass, Teflon ®
• Cooling Water Connection Diameter: Cooling Cartridge: Outer Diameter 12 mm Hose Port
• Gas connection bore: Electric part Air purge: Outer diameter 6mm One-touch joint
• Aluminum block dimensions: 60 mm outer diameter for reaction vessels (without test tube adapter installed)
• Operating ambient temperature range: 5 ~ 35 degrees C
• External dimensions (mm)/Mass: 475 W x 383 D x 290 H/26 kg
• Power input/voltage: 13 A, 1300 VA/AC 100 V 50/60 Hz
• Configuration:
• Reaction vessel related parts: Sold separately
• Drip-Proof Cover: Product Code No. 228010 (x 4 pieces)
• Temperature control/stirring section: PPV- CTRL1 type product code No. 227230
• *Performance is measured at 20 degrees Celsius, rated supply voltage, no load, and when using a cooling water circulator (Cooling capacity: 330 W, at -30 degrees C).
• *To adjust the temperature, a connection with a cooling water circulator CA -1116 A/1330: -10 degrees C or PFR -1000 + PFP -1000 (refrigerant: ethanol -27 degrees C or higher) is required.
• *A connection to a tap or cold water circulator ACE -2000 is required for reflux.
• *Test tube adapter, drip-proof cover, reaction vessel, stirrer and other parts are sold separately.
• *Manifold PPV Model -34 M Product Code No. 228110, Stand Unit Product Code No. 228150 and Cooling Hose Set are sold separately.
• Accessories:
• Temperature control/stirring section: fuse (2)
• Code: 254870